Kocaeli University / European Credit Transfer System (ECTS)

Name of Lecturer(s)

Lecturer Ufuk AKKAN
Lecturer Ayşe Gül BALOĞLU
Lecturer Dr. Meryem PİR

Learning Outcomes of the Course Unit
Program Competencies-Learning Outcomes Relation

Learning Outcomes of the Course Unit

1) The operation of Infrared Spectrophotometer
2) Calibration and sample preparation skills of Infrared Spectrophotometer
3) Interpretation of Infrared Spectroscopy
4) Give a brief discussion of NMR and Mass Spectroscopy

Program Competencies-Learning Outcomes Relation

		Program Competencies
		1	2	3	4	5	6	7	8	9	10
Learning Outcomes
	1	High	Middle	High	High	No relation	No relation	No relation	No relation	No relation	Low
	2	High	Middle	High	High	No relation	No relation	No relation	No relation	No relation	Low
	3	High	Middle	High	High	No relation	No relation	No relation	No relation	No relation	Low
	4	High	Middle	High	High	No relation	No relation	No relation	No relation	No relation	Low

Mode of Delivery

Face to Face

Prerequisites and Co-Requisites

None

Recommended Optional Programme Components

Instrumental Analysıs I

Course Contents

Infrared spectroscopic analysis, principles of infrared spectroscopy prepare samples and interpret infrared spectra, prepare a solution of an organic liquid or solid and obtain its spectrum. Nuclear magnetic spectroscopic analysis, principles of nuclear magnetic resonance spectroscopy, describe the process for obtaining spectra and evaluate the results. Mass spectroscopic analysis, principles of mass spectroscopy describe the process of obtaining spectra and evaluate the results, qualitative organic analysis.

Weekly Schedule

1) General information about courses and course textbooks, what is spectroscopy, spectroscopic methods are?
2) Red Cross (Infrared) spectroscopy, nuclear magnetic resonance (NMR); Mass spectrometer (MASS) brief information about
3) Where IR radiation in the wavelength range, vibrations, Hooke's equation.
4) Beyond red spectroscopy, the basic components, techniques of spectrum (solid, liquid and gas samples)
5) Explanation of the infrared spactral region, the effects that change the group frequency (inductive effect, resonance effect, non-molecular reactions, solvent effects, the band splitting, functional group interactions, the ring size)
6) Unsaturation degree, the first approach for evaluation of IR spectroscopy, general rules, functional groups of the region, the fingerprint region
7) IR spectrum for functional group compounds are examples of comments about the mutual
8) Midterm examination/Assessment
9) Running the IR device (an unknown organic solid and liquid materials fron the IR spectrum and the structure of matter)
10) Nuclear magnetic resonance spectroscopy of organic compounds in the analysis of the structure (the basis of NMR, resonance, relaxation)
11) Chemical shift, factors affecting chemical shift, substituents, aromatic compounds to effect of chemical shift, standart item on NMR
12) The influence of chemical shift of more bonds, spin-spin interaction, the disclosure of peaks according to the Pascal triangle
13) Second-order spectra, the factors of effect that spin-spin interactions
14) The interaction of a proton with other protons (doublet of doublet, doublet of triplet, doublet of quartet, doublet of doublet triplet)
15) Mass spektroscopy (MASS) policies, procedures and results of spectrum acquisition
16) Final examination

Planned Learning Activities and Teaching Methods

1) Lecture
2) Question-Answer
3) Brain Storming
4) Case Study

Assessment Methods and Criteria

Contribution of Midterm Examination to Course Grade	30%
Contribution of Final Examination to Course Grade	70%
Total	100%

Language of Instruction

Turkish

Work Placement(s)

Not Required

Course Unit Title	Course Unit Code	Type of Course Unit	Level of Course Unit	Year of Study	Semester	ECTS Credits
Instrumental Analysis II	KTP230	Elective	Associate degree	2	Spring	3