Instrumental Analysis Methods II

Mode of Delivery

Face to Face

Prerequisites and Co-Requisites

None

Recommended Optional Programme Components

Instrumental Analysıs I

Course Contents

Infrared spectroscopic analysis, principles of infrared spectroscopy prepare samples and interpret infrared spectra, prepare a solution of an organic liquid or solid and obtain its spectrum. Nuclear magnetic spectroscopic analysis, principles of nuclear magnetic resonance spectroscopy, describe the process for obtaining spectra and evaluate the results. Mass spectroscopic analysis, principles of mass spectroscopy describe the process of obtaining spectra and evaluate the results, qualitative organic analysis.

Weekly Schedule

1) General information about courses and course textbooks, what is spectroscopy, spectroscopic methods are?
2) Red Cross (Infrared) spectroscopy, nuclear magnetic resonance (NMR), Mass Spectrometer (MASS), brief information about
3) Where IR radiation in the wavelength range, vibrations, Hooke's equation
4) Beyond red spectroscopy, the basic components, techniques of spectrum (solid, liquid and gas sample)
5) Explanation of the infrared spectral region, the effects that change the group frequency (inductive effect, resonance effect, non-molecular reactions, solvent effects, the band splitting, functional group interactions, the ring size)
6) Unsaturation degree, the first approach for evaluation of IR spectroscopy, general rules, functional groups of the region, the fingerprint region
7) IR spectrum for functional group compounds are examples of comments about the mutual
8) Midterm examination/Assessment
9) Running the IR device (an unknown organic solid and liquid materials from the IR spectrum and the structure of matter)
10) Nuclear magnetic resonance spectroscopy of organic compounds in the analysis of the structure (the basis of NMR, resonance, relaxation)
11) Chemical shift, factors affecting chemical shift, substituents, aromatic compounds, to the effect of chemical shift, NMR is also a standard item
12) The influence of chemical shift of more bonds, spin-spin interaction, the disclosure of peaks according to the Pascal triangle
13) Second-order spectra, the factors that affect spin-spin interaction of
14) The interaction of a proton with other protons (dubletin dublete, dubletin triplet, dubletin-quartets, the dubletin dubletinin triplet)
15) Mass (MASS) spektrskopisi policies, procedures and results of spectrum acquisition
16) Final examination

Recommended or Required Reading

Planned Learning Activities and Teaching Methods

Assessment Methods and Criteria

Language of Instruction

Turkish

Work Placement(s)

Not Required