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Course Unit Title Course Unit Code Type of Course Unit Level of Course Unit Year of Study Semester ECTS Credits
Org. Structural Analysis With Nmr Spect. KIM613 Elective Doctorate degree 1 Fall 8

Name of Lecturer(s)

Prof. Dr. Hikmet AĞIRBAŞ
Prof. Dr. Cavit UYANIK
Prof. Dr. Mehmet YILMAZ
Associate Prof. Dr. Selahaddin GÜNER

Learning Outcomes of the Course Unit

1) Explain stereochemistry and make structural analysis of organic molecules by using 2 and 3 dimensional NMR techniques
2) Explain Homo Cosy
3) Explain Hetcorr spectrum
4) Explain inadaquate spectrum
5) Explain Noesy spectrum

Program Competencies-Learning Outcomes Relation

  Program Competencies
1 2 3 4
Learning Outcomes
1 Middle No relation No relation No relation
2 Middle No relation No relation No relation
3 Middle No relation No relation No relation
4 Middle No relation No relation No relation
5 Middle No relation No relation No relation

Mode of Delivery

Face to Face

Prerequisites and Co-Requisites

None

Recommended Optional Programme Components

organic chemistry-1 and organic chemistry-2

Course Contents

Candidates are provided with in-depth knowledge on 1H NMR ve 13C NMR spectra, spin decoupling, nuclear overhauser effect (NOE), two dimention NMR, 1H-1H Cosy (homo nuclear) spectra, 13C-1H Cosy (hetero nuclear) spectra, NOE different spectra, Noesy spectra, inadequate spectra, 3-D and 4-D NMR spectra, examples and problems.

Weekly Schedule

1) 1H NMR spectra,
2) 13C NMR spectra,
3) Spin coupling and decoupling
4) Nuclear Overhauser effect (NOE)
5) 1H -1H COSY (HOMO Nuclear) spectrumu
6) 13C -1H COSY (Hetero Nuclearr) spectrumu
7) NOE different spectra
8) Midterm examination/Assessment
9) Inadequate spectra,
10) 3D NMR spectra,
11) 4-D NMR spectra
12) Problem solving
13) Problem solving
14) Mix Problemler
15) mix problems
16) Final examination

Recommended or Required Reading

Planned Learning Activities and Teaching Methods

1) Lecture
2) Discussion
3) Demonstration
4) Group Study
5) Problem Solving


Assessment Methods and Criteria

Contribution of Midterm Examination to Course Grade

50%

Contribution of Final Examination to Course Grade

50%

Total

100%

Language of Instruction

Turkish

Work Placement(s)

Not Required