Nmr Spectroscopy of Polymers
Polymer Science and Technology
Institute of Natural and Applied Sciences
Third Cycle (Doctorate Degree)
| Course Unit Title | Course Unit Code | Type of Course Unit | Level of Course Unit | Year of Study | Semester | ECTS Credits |
|---|---|---|---|---|---|---|
| Nmr Spectroscopy of Polymers | PST623 | Elective | Doctorate degree | 1 | Fall | 8 |
Name of Lecturer(s)
Prof. Dr. Olcay MERT
Assistant Prof. Dr. Serap MERT
Learning Outcomes of the Course Unit
1) to identify the differences between polymers of NMRs
2) to comment of NMRs for sample polymers
Program Competencies-Learning Outcomes Relation
| Program Competencies | |||||
| 1 | 2 | 3 | 4 | ||
| Learning Outcomes | |||||
| 1 | Middle | Middle | Middle | Middle | |
| 2 | Middle | Middle | Middle | Middle | |
Mode of Delivery
Face to Face
Prerequisites and Co-Requisites
None
Recommended Optional Programme Components
Not Required
Course Contents
Introduction to NMR, Experimental Methods, The Solution Characterization of Polymers, The Solid-State NMR of Polymers, Copolymers, NMR For The Study Of Polymerization Reactions, Applications of Two Dimensional NMR Spectroscopy of Polymers, Dynamics of Polymers, Online SEC/NMR Analysis of Polymers
Weekly Schedule
1) Introduction to NMR (Basic Principles of NMR, Chemical Shifts and Polymer Structure, ...)2) Experimental Methods
3) The Solution Characterization of Polymers- Polymer Microstructure (Regioisomerism, steriochemical isomerism, geometric isomerism, branching and endgroups, chain architecture)
4) The Solution Characterization of Polymers - Spectral Assignments in Polymers (Model Compounds and Polymers, Polymer Chain Statistics, Chemical Shift Calculations)
5) The Solution Characterization of Polymers - Stereochemical Characterization of Polymers (The Observation of Stereochemical Isomerism and Resonance Assignments for Stereosequences)
6) The Solid-State NMR of Polymers - Chain Conformation in Polymers
7) The Solid-State NMR of Polymers - Structure and Morphology in Polymers
8) Midterm
9) Copolymers
10) NMR For The Study Of Polymerization Reactions (I)
11) NMR For The Study Of Polymerization Reactions (II)
12) Applications of Two Dimensional NMR Spectroscopy of Polymers
13) NMR Relaxation of Polymers
14) Dynamics of Polymers
15) Online SEC/NMR Analysis of Polymers
16) Final
Recommended or Required Reading
Planned Learning Activities and Teaching Methods
1) Lecture
2) Question-Answer
3) Discussion
4) Problem Solving
Assessment Methods and Criteria
Contribution of Midterm Examination to Course Grade |
50% |
|---|---|
Contribution of Final Examination to Course Grade |
50% |
Total |
100% |
Language of Instruction
Turkish
Work Placement(s)
Not Required